湿法涂层工艺对阻燃商标布形貌及阻燃性能的影响

doi:10.19398/j.att.202101027

现代纺织技术 ›› 2022, Vol. 30 ›› Issue (2): 178-183.DOI: 10.19398/j.att.202101027

湿法涂层工艺对阻燃商标布形貌及阻燃性能的影响

蒋继康¹, 虞一浩², 符晔², 雷鹏飞², 戚栋明¹, 陈智杰³()

1.浙江理工大学先进纺织材料与制备技术教育部重点实验室,杭州 310018
2.浙江凯瑞博科技有限公司,浙江湖州 313100
3.温州职业技术学院聚合物材料及机电产品表面改性技术研究重点实验室,浙江温州 325035

收稿日期:2021-01-22 出版日期:2022-03-10 网络出版日期:2021-08-05
通讯作者: 陈智杰,E-mail: chenzhijie5262@163.com
作者简介:蒋继康(1996-),男,湖北潜江人,硕士研究生,主要从事无机填料粒子的改性及其在湿法涂层方面的研究。
基金资助:
浙江省重点研发项目(2021C01077);温州职业技术学院重大科技项目(WZY2020002,);温州市科技局基础性科研项目(G2020025)

Effect of wet coating process on the morphology and flame-retardant properties of anti-flaming trademark fabric

JIANG Jikang¹, YU Yihao², FU Ye², LEI Pengfei², QI Dongming¹, CHEN Zhijie³()

1. Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Zhejiang Sci-Tech University, Hangzhou 310018, China
2. Zhejiang King Label Technology Co., Ltd., Huzhou 313100, China
3. Key Laboratory of Surface Modification of Polymer Materials and Mechanical and Electrical Products, Wenzhou Polytechnic, Wenzhou 325035, China

Received:2021-01-22 Published:2022-03-10 Online:2021-08-05

摘要/Abstract

摘要：

为提高聚酰胺湿法涂层织物的阻燃性能,将阻燃剂9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物(DOPO)作为填料添加于聚酰胺湿法涂层浆料中。研究以DOPO为填料的聚酰胺湿法涂层工艺(涂层浆料放置时间、烘焙温度、相转变时间)对所制涂层织物服用性能和阻燃性能的影响,进而得出最佳湿法涂层工艺。结果表明:DOPO加入聚酰胺湿法涂层浆料后,商标布的最佳涂层浆料黏度为0.7 Pa·s,最佳相转变时间为15 s,最佳烘焙温度为100 ℃,所制阻燃商标布具有较佳的阻燃效果和手感。

关键词: 湿法涂层, 聚酰胺涂层, 阻燃, 商标布, 手感

Abstract:

In order to enhance the flame retardant properties of PA wet coating fabrics, the flame retardant 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO)was selected as a filler to add into the wet coated polyamide slurry. This paper is focused on studying the impact of wet coated polyamide with DOPO as the filler (the storage time, baking temperature, phase transformation time of coating slurry)on the wearability and flame retardant properties of the coated fabric, so as to obtain the optimal wet coating process. The results reveal that after DOPO is added to the polyamide wet coating slurry, the optimal coating slurry viscosity of the trademark fabric is 0.7 Pa·s, the optimal phase transformation time is 15 s, and the optimal baking temperature is 100 ℃. The anti-flaming trademark fabric can achieve better flame-retardant efficiency and hand feeling.

Key words: wet coating, polyamide coating, flame retardant, trademark fabric, hand feeling

中图分类号:

TS195

蒋继康, 虞一浩, 符晔, 雷鹏飞, 戚栋明, 陈智杰. 湿法涂层工艺对阻燃商标布形貌及阻燃性能的影响[J]. 现代纺织技术, 2022, 30(2): 178-183.

JIANG Jikang, YU Yihao, FU Ye, LEI Pengfei, QI Dongming, CHEN Zhijie. Effect of wet coating process on the morphology and flame-retardant properties of anti-flaming trademark fabric[J]. Advanced Textile Technology, 2022, 30(2): 178-183.

图/表 6

图1 放置时间对浆料粘度和涂层厚度的影响

Fig.1 Effect of placement time on slurry viscosity and coating thickness

图2 浆料粘度对涂层极限氧指数和硬挺度的影响

Fig.2 Effect of slurry viscosity on limiting oxygen index and stiffness of coating

图3 不同相转变时间下形成的聚酰胺涂层膜表面形貌

Fig.3 Surface morphology of polyamide coatings formed at different phase transition times

图4 相转变时间对涂层硬挺度和厚度的影响

Fig.4 Effect of phase transition time on stiffness and thickness of coating

图5 不同烘焙温度制备的涂层膜表面形貌

Fig.5 Surface morphology of coating film prepared at different baking temperatures

图6 不同烘焙温度对涂层织物的极限氧指数和硬挺度的影响

Fig.6 Effects of different baking temperatures on limiting oxygen index and stiffness of coated fabrics

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湿法涂层工艺对阻燃商标布形貌及阻燃性能的影响

Effect of wet coating process on the morphology and flame-retardant properties of anti-flaming trademark fabric

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